| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
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; Side reactions |
Synthesis of adamantylideneadamantane from adamantanone |
| Reaction type: | McMurry reaction, reductive coupling, alkenesynthesis |
| Substance classes: | ketone, alkene |
| Techniques: | working with cover gas, adding dropwise with a piston-operated pipette, adding dropwise with an addition funnel, stirring with magnetic stir bar, heating under reflux, shaking out, extracting, Abfiltrieren, evaporating with rotary evaporator, recrystallizing, use of an ice cooling bath, heating with oil bath |
| Degree of difficulty: | Difficult |