| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
1H-NMR |
| 1H-NMR: crude product | |||
| 250 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 0.99 | t | 3 H | 4-CH3 (butyl) |
| 1.13 | t | 3 H | 3-CH3 (propanoic acid residue) |
| 1.38 | m | 2 H | 3-CH2 (butyl) |
| 1.60 | m | 2 H | 2-CH2 (butyl) |
| 2.31 | q | 2 H | 2-CH2 (propanoic acid residue) |
| 4.06 | t | 2 H | 1-CH2 (butyl) |
| 1.42 | CH2 (cyclohexane) | ||
| 1H-NMR: Propionic acid butyl ester | |||
| 250 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 0.99 | t | 3 H | 4-CH3 (butyl) |
| 1.13 | t | 3 H | 3-CH3 (propanoic acid residue) |
| 1.38 | m | 2 H | 3-CH2 (butyl) |
| 1.60 | m | 2 H | 2-CH2 (butyl) |
| 2.31 | q | 2 H | 2-CH2 (propanoic acid residue) |
| 4.06 | t | 2 H | 1-CH2 (butyl) |
| 1.42 | CH2 (cyclohexane) | ||