| Überblick |
| Synthesevorschrift |
| Operationsschema |
| Stoffe |
| Geräte |
| Bewertung |
| Analytik |
| - Chromatogramm |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| Betriebsanweisungen |
|
|
|
; Nebenreaktionen |
13C-NMR |
| 13C-NMR: (-)-Menthol und (+)-Neomenthol, Mischung | |||
| 400 MHz, CDCl3 | |||
| delta [ppm] | Zuordnung | ||
| 15.97 | CH3 (Isopropyl), (Menthol) | ||
| 20.95 | CH3 (Isopropyl), (Menthol) | ||
| 22.15 | CH3 (mEthyl), (Menthol) | ||
| 23.02 | C3 (Cyclohexan), (Menthol) | ||
| 25.67 | CH (Isopropyl), (Menthol) | ||
| 31.57 | C5 (Cyclohexan), (Menthol) | ||
| 34.48 | C4 (Cyclohexan), (Menthol) | ||
| 44.97 | C6 (Cyclohexan), (Menthol) | ||
| 50.01 | C2 (Cyclohexan), (Menthol) | ||
| 71.36 | C1 (CHOH), (Menthol) | ||
| 20.64 | CH3 (Isopropyl), (Neomenthol) | ||
| 21.10 | CH3 (Isopropyl), (Neomenthol) | ||
| 22.28 | CH3 (mEthyl), (Neomenthol) | ||
| 24.09 | C3 (Cyclohexan), (Neomenthol) | ||
| 25.72 | CH (Isopropyl), (Neomenthol) | ||
| 29.05 | C5 (Cyclohexan), (Neomenthol) | ||
| 34.99 | C4 (Cyclohexan), (Neomenthol) | ||
| 42.50 | C6 (Cyclohexan), (Neomenthol) | ||
| 47.88 | C2 (Cyclohexan), (Neomenthol) | ||
| 67.57 | C1 (CHOH), (Neomenthol) | ||
| 76.5-77.5 | CDCl3 | ||