| Überblick |
| Synthesevorschrift |
| Operationsschema |
| Stoffe |
| Geräte |
| Bewertung |
| Analytik |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| Betriebsanweisungen |
| + |
|
|
|
; Nebenreaktionen |
13C-NMR |
| 13C-NMR: Rohprodukt | |||
| 75.5 MHz, MeOD | |||
| delta [ppm] | Zuordnung | ||
| 22.5 | |||
| 25.9 | |||
| 28.0 | |||
| 39.1 | |||
| 52.7 | |||
| 62.0 | |||
| 65.2 | CH2 Benzyl | ||
| 66.2 | |||
| 69.7 | |||
| 117.5 | |||
| 121.4 | |||
| 124.2 | |||
| 126.1 | |||
| 128.8 | |||
| 129.1 | |||
| 130.3 | |||
| 131.1 | |||
| 131.7 | |||
| 134.9 | |||
| 138.7 | |||
| 147.6 | |||
| 148.7 | |||
| 151.0 | |||
| 47-50 | CH3OD | ||
| 13C-NMR: (-)-N-Benzylcinchonidiniumchlorid | |||
| 75.5 MHz, MeOD | |||
| delta [ppm] | Zuordnung | ||
| 22.5 | |||
| 25.9 | |||
| 28.0 | |||
| 39.1 | |||
| 52.7 | |||
| 62.0 | |||
| 65.2 | CH2 Benzyl | ||
| 66.2 | |||
| 69.7 | |||
| 117.5 | |||
| 121.4 | |||
| 124.2 | |||
| 126.1 | |||
| 128.8 | |||
| 129.1 | |||
| 130.3 | |||
| 131.1 | |||
| 131.7 | |||
| 134.9 | |||
| 138.7 | |||
| 147.6 | |||
| 148.7 | |||
| 151.0 | |||
| 47-50 | CH3OD | ||