| Overview |
| Instructions |
| Operating scheme |
| Substances |
| - Substances required |
| - Substances produced |
| - Data availability |
| - Effect factors TRGS 600 |
| - Stoichiometry |
| Equipment |
| Evaluation |
| Analytics |
|
|
| + |
| + |
|
; Side reactions |
Substances required |
| Educts | Amount | Risk | Safety | ||||||
|---|---|---|---|---|---|---|---|---|---|
| Toluene |
|
53 mL | H225 H361d H304 H373 H315 H336 | P210 P281 P301 + 310 P331 P302 + 352 P308 + 313 | |||||
| Reagents | Amount | Risk | Safety | ||||||
| Nitric acid (conc.) |
|
53 mL | H272 H314 | P220 P280 P305 + 351 + 338 P310 | |||||
| Catalyst | Amount | Risk | Safety | ||||||
| Sulfuric acid (conc.) |
|
61 mL | H314 H290 EUH- | P280 P301 + 330 + 331 P305 + 351 + 338 P309 + 310 | |||||
| Solvents | Amount | Risk | Safety | ||||||
| Cyclohexane |
|
280 mL | H225 H304 H315 H336 H410 | P210 P233 P240 P273 P301 + 310 P302 + 352 P331 P403 + 235 | |||||
| Water |
|
590 mL | H- EUH- | P- | |||||
| Ethanol |
|
15 mL | H225 H302 H371 EUH- | P210 P260 | |||||
| Methanol |
|
15 mL | H225 H331 H311 H301 H370 | P210 P260 P280 P301 + 310 P311 | |||||
| Others | Amount | Risk | Safety | ||||||
| Ice |
|
250 g | H- EUH- | P- | |||||
| Sodium hydrogen carbonate |
|
~ 4 g | |||||||
| Sodium sulfate |
|
~ 20 g | |||||||
| Sodium hydroxide (2 N) |
|
500 mL | H314 EUH- | P280 P305 + 351 + 338 P310 | |||||
| Solvents for analysis | Amount | Risk | Safety | ||||||
| Methanol |
|
3 mL | H225 H331 H311 H301 H370 | P210 P260 P280 P301 + 310 P311 | |||||
| n-Hexane |
|
? | H225 H361f H304 H373 H315 H336 H411 | P210 P261 P273 P281 P301 + 310 P331 | |||||
| Acetic acid ethyl ester |
|
? | H225 H319 H336 EUH066 | P210 P261 P305 + 351 + 338 |
