| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
1H-NMR |
| 1H-NMR: crude product | |||
| 400 MHz, CDCl3, TMS | |||
| delta [ppm] | mult. | atoms | assignment |
| 7.76-7.80 | t | 1 H | 5-H |
| 8.23-8.25 | m | 1 H | 6-H |
| 8.48-8.51 | m | 1 H | 4-H |
| 8.72-8.73 | m | 1 H | 2-H |
| 10.13 | s | 1 H | CHO |
| 7.26 | CHCl3 | ||
| 1H-NMR: 3-Nitrobenzaldehyde | |||
| 400 MHz, CDCl3, TMS | |||
| delta [ppm] | mult. | atoms | assignment |
| 7.76-7.80 | t | 1 H | 5-H |
| 8.23-8.25 | m | 1 H | 6-H |
| 8.48-8.51 | m | 1 H | 4-H |
| 8.72-8.73 | m | 1 H | 2-H |
| 10.13 | s | 1 H | CHO |
| 7.26 | CHCl3 | ||