| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
1H-NMR |
| 1H-NMR: crude product | |||
| 400 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.43 | t | 3 H | CH3 ethyl |
| 2.13 | s | 3 H | CH3 acetyl |
| 4.03 | q | 2 H | CH2 ethyl |
| 6.77 | dd | 1 H | 5-H |
| 7.35 | dd | 1 H | 6-H |
| 7.68 | dd | 1 H | 2-H |
| 8.13 | s | 1 H | NH |
| 7.26 | CHCl3 | ||
| 1H-NMR: 3-Bromo-4-ethoxyacetanilide | |||
| 400 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.43 | t | 3 H | CH3 ethyl |
| 2.13 | s | 3 H | CH3 acetyl |
| 4.03 | q | 2 H | CH2 ethyl |
| 6.77 | dd | 1 H | 5-H |
| 7.35 | dd | 1 H | 6-H |
| 7.68 | dd | 1 H | 2-H |
| 8.13 | s | 1 H | NH |
| 7.26 | CHCl3 | ||