| Overview |
| Instructions |
| Operating scheme |
| Substances |
| - Substances required |
| - Substances produced |
| - Data availability |
| - Effect factors TRGS 600 |
| Equipment |
| Evaluation |
| Analytics |
|
|
|
; Side reactions |
Substances required |
| Educts | Amount | Risk | Safety | ||||||
|---|---|---|---|---|---|---|---|---|---|
| 3-Phenylpropionic acid | 1.5 g | ||||||||
| Reagents | Amount | Risk | Safety | ||||||
| Polyphosphoric acid |
|
10 g | H314 | P280 P305 + 351 + 338 P310 | |||||
| Solvents | Amount | Risk | Safety | ||||||
| tert-Butyl methyl ether |
|
30 mL | H225 H315 | P210 | |||||
| n-Heptane |
|
4500 mL | H225 H315 H304 H336 H410 EUH- | P210 P261 P273 P301 + 310 P331 P501 | |||||
| Acetic acid ethyl ester |
|
500 mL | H225 H319 H336 EUH066 | P210 P261 P305 + 351 + 338 | |||||
| Water |
| H- EUH- | P- | ||||||
| Others | Amount | Risk | Safety | ||||||
| Sodium hydroxide, 5 percent |
|
5 mL | H314 EUH- | P280 P305 + 351 + 338 P310 | |||||
| Magnesium sulfate |
|
~1 g | |||||||
| Silica gel |
|
ca. 520 g | |||||||
| Ice |
|
30 g | H- EUH- | P- | |||||
| Solvents for analysis | Amount | Risk | Safety | ||||||
| Cyclohexane |
| H225 H304 H315 H336 H410 | P210 P233 P240 P273 P301 + 310 P302 + 352 P331 P403 + 235 | ||||||
| Acetic acid ethyl ester |
| H225 H319 H336 EUH066 | P210 P261 P305 + 351 + 338 |
