| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| + |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 100 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 31.41 | CH3 | ||
| 34.24 | C(CH3)3 | ||
| 124.88 | C2, C3, C5, C6 | ||
| 148.00 | C1, C4 | ||
| 76.5-77.5 | CDCl3 | ||
| 34.99 | C(CH3)3 byproduct | ||
| 119.45 | C2, C4, C6 (byproduct) | ||
| 149.93 | C1, C3, C5 (byproduct) | ||
| 13C-NMR: 1,4-Di-tert-butylbenzene | |||
| 100 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 31.41 | CH3 | ||
| 34.24 | C(CH3)3 | ||
| 124.88 | C2, C3, C5, C6 | ||
| 148.00 | C1, C4 | ||
| 76.5-77.5 | CDCl3 | ||
| 34.99 | C(CH3)3 byproduct | ||
| 119.45 | C2, C4, C6 (byproduct) | ||
| 149.93 | C1, C3, C5 (byproduct) | ||