| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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|
; Side reactions |
Chromatogram |
| TLC: crude product | |
| TLC layer | Polygram SilG/UV precoated TLC layer; 0.2 mm; silica gel; Macherey & Nagel |
| mobile phase | cyclohexane / EtOAc = 95 : 5 |
| staining reagent | Vaughn's reagent or iodine vapor |
| Rf (product) | 0.51 |