NOP-Nr:
Alternative:
4010
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
+
Sc(OTf)
3
+
; Side reactions
Synthesis of p-methoxyacetophenone from anisole
Reaction type:
electrophilic substitution of aromatics, Friedel-Crafts acylation, reaction of the carbonyl group in carboxylic acid derivatives
Substance classes:
aromatics, carboxylic acid anhydride, acid catalyst
Techniques:
working with cover gas, adding dropwise with an addition funnel, shaking out, extracting, filtering, distilling under reduced pressure, evaporating with rotary evaporator, stirring with magnetic stir bar, heating with oil bath
Degree of difficulty:
Medium
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pages/experiment.php: November 09, 2022
views/overview.php: November 09, 2022