| Overview |
| Instructions |
| Operating scheme |
| Substances |
| - Substances required |
| - Substances produced |
| - Data availability |
| - Effect factors TRGS 600 |
| - Stoichiometry |
| Equipment |
| Evaluation |
| Analytics |
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| + |
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; Side reactions |
Substances required |
| Educts | Amount | Risk | Safety | ||||||
|---|---|---|---|---|---|---|---|---|---|
| Anisole |
|
5.4 g | H226 H315 H319 EUH- | P305 + 351 + 338 | |||||
| Acetic anhydride |
|
5.1 g | H226 H302 H314 H332 EUH- | P280 P305 + 351 + 338 P310 | |||||
| Catalyst | Amount | Risk | Safety | ||||||
| Scandium(III) triflate |
|
4.90 g | H315 H319 H335 EUH- | P261 P305 + 351 + 338 | |||||
| Solvents | Amount | Risk | Safety | ||||||
| Nitromethane |
|
60 mL | H226 H302 EUH- | P- | |||||
| tert-Butyl methyl ether |
|
140 mL | H225 H315 | P210 | |||||
| Water |
|
150 mL | H- EUH- | P- | |||||
| Others | Amount | Risk | Safety | ||||||
| Magnesium sulfate |
|
3 g | |||||||
| Sodium chloride |
|
40 g | |||||||
| Nitrogen |
|
? | H280 | P410 + 403 | |||||
| Solvents for analysis | Amount | Risk | Safety | ||||||
| n-Heptane |
|
? | H225 H315 H304 H336 H410 EUH- | P210 P261 P273 P301 + 310 P331 P501 | |||||
| Acetic acid ethyl ester |
|
? | H225 H319 H336 EUH066 | P210 P261 P305 + 351 + 338 |
