| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
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Acid catalyzed acetalisation of acetoacetic acid ethyl ester with ethanediol to the corresponding 1,3-dioxolane |
| Reaction type: | reaction of the carbonyl group in ketones, acetalisation |
| Substance classes: | ketone, alcohol, acetal, protecting group, acid catalyst |
| Techniques: | removal of water by azeotropic distillation, stirring with KPG stirrer, filtering, evaporating with rotary evaporator, distilling under reduced pressure, fractionating column distillation, rectifying, heating with oil bath, stirring with magnetic stir bar |
| Degree of difficulty: | Easy |