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Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
Acetoacetic acid ethyl ester + 1,2-Ethanediol
montmorillonite
K-10
reacts to
 2-Methyl-1,3-dioxolane-2-acetic acid ethyl ester + Water ; Side reactions

Equipment

Batch scale: 0.01 mol 0.2 mol 1 mol Acetoacetic acid ethyl ester
round bottom flask 100 mL round bottom flask 100 mL Soxhlet extractor 30 mL Soxhlet extractor 30 mL
extraction cone extraction cone reflux condenser reflux condenser
oil bath oil bath heatable magnetic stirrer with magnetic stir bar heatable magnetic stirrer with magnetic stir bar
microdistillation apparatus microdistillation apparatus vacuum pump vacuum pump
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