Reduction of L-(-)-menthone with lithium aluminum hydride to an isomeric mixture of (-)-menthol and (+)-neomenthol
Reaction type:
reaction of the carbonyl group in ketones, reduction, stereoselective addition
Substance classes:
ketone, alcohol, complex metal hydride, natural product
Techniques:
working with moisture exclusion, stirring with KPG stirrer, adding dropwise with an addition funnel, heating under reflux, filtering, evaporating with rotary evaporator, distilling under reduced pressure, use of a cooling bath, heating with oil bath