| Overview |
| Instructions |
| Operating scheme |
| Substances |
| - Substances required |
| - Substances produced |
| - Data availability |
| - Effect factors TRGS 600 |
| Equipment |
| Evaluation |
| Analytics |
|
|
|
; Side reactions |
Substances produced |
| Products | Amount | Risk | Safety | |||||
|---|---|---|---|---|---|---|---|---|
| Cyclohexancarboxylic acid |
|
7.77 g | H315 H318 H335 EUH- | P261 P280 P305 + 351 + 338 | ||||
| Byproducts | Amount | Risk | Safety | |||||
| Cyclohexane |
| H225 H304 H315 H336 H410 | P210 P233 P240 P273 P301 + 310 P302 + 352 P331 P403 + 235 | |||||
| Cyclohexene |
| H225 H302 H304 H311 | P210 P280 P301 + 310 P312 P331 | |||||
| Cyclohexanol |
| H302 H315 H332 H335 EUH- | P261 | |||||
| Bicyclohexyl |
| H400 EUH- | P273 | |||||
| Magnesium bromide |
| H315 H319 H335 EUH- | P261 P305 + 351 + 338 | |||||
| Cyclohexylmagnesium bromide |
|
| Waste | Disposal |
|---|---|
| aqueous phase after shaking out with diethyl ether of the acidified reaction solution | solvent water mixtures, containing halogens |
| aqueous phase after shaking out with diethyl ether of acidified aqueous phase | solvent water mixtures, containing halogens |
| diethyl ether phase after shaking out with aqueous NaOH | organic solvents, halogen free |
| distillation residues | solid waste, free from mercury |
| sodium sulfate | solid waste, free from mercury |
| diethyl ether phase after shaking out of alkaline aqueous phase | solvents for rectification |
| evaporated diethyl ether from crude product | solvents for rectification |