| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| + |
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; Side reactions |
Chromatogram |
| GC: pure product | |
| column | Zebron ZB-1, L=15 m, d=0.25 mm, film=0.25 µm |
| inlet | injector: 280°C, split injection, 0.1 µl |
| carrier gas | H2, pre-column pressure 150 kPa |
| oven | 30°C (2 min), 8°C/min --> 250°C (2 min) |
| detector | FID, 300°C, H2 25.1 mL/min, synth. air 393 mL/min |
| integration | percent concentration calculated from relative peak area |