NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
+
NaOH,Pr
3
N
+
; Side reactions
1
H-NMR
1
H-NMR: crude product
500 MHz, CDCl
3
delta [ppm]
mult.
atoms
assignment
1.12-1.36
m
4 H
C4-H, C5-H
1.61-1.71
m
4 H
C3-H, C6-H
1.88-1.98
m
2 H
C1-H, C2-H
7.26
s
1 H
CHCl
3
1
H-NMR: 7,7-Dichlorobicyclo[4.1.0]heptane
500 MHz, CDCl
3
delta [ppm]
mult.
atoms
assignment
1.12-1.36
m
4 H
C4-H, C5-H
1.61-1.71
m
4 H
C3-H, C6-H
1.88-1.98
m
2 H
C1-H, C2-H
7.26
s
1 H
CHCl
3
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pages/experiment.php: November 09, 2022
views/hnmr.php: November 09, 2022