| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| + |
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; Side reactions |
1H-NMR |
| 1H-NMR: trans-5-Norbornene-2,3-dicarboxylic acid | |||
| 250 MHz, Me2C=O-d6 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.41 | ddd (2J = 8.5 Hz; 3J = 4.0 Hz; J = 1.8 Hz) | 1 H | 7-H (CH2) |
| 1.61 | m (2J = 8.5 Hz) | 1 H | 7-H (CH2) |
| 2.62 | dd | 1 H | 2-H, 3-H (CH-COOH) |
| 3.12 | m | 1 H | 1-H, 4-H (CH) |
| 3.24 | m | 1 H | 1-H, 4-H (CH) |
| 3.35 | dd (3J = 4.6 Hz; 3J = 4.1 Hz) | 1 H | 2-H, 3-H (CH-COOH) |
| 6.09 | dd (3J = 5.8 Hz; J = 2.7 Hz) | 1 H | 5-H, 6-H (CH=CH) |
| 6.29 | dd (3J = 5.8 Hz; J = 3.0 Hz) | 1 H | 5-H, 6-H (CH=CH) |
| 9 | broad s | 2 H | COOH |
| 2.09 | Me2C=O | ||