| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
1H-NMR |
| 1H-NMR: crude product | |||
| 250 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.23 | t (3J = 7.2 Hz) | 6 H | CH3 ethyl |
| 3.45 | m | 2 H | 11-H, 12-H (-CH-COO-) |
| 4.08 | m | 4 H | CH2 ethyl |
| 4.75 | m | 2 H | 9-H, 10-H |
| 7.09-7.38 | m | 8 H | CH (arom.) |
| >7.4 | CH (arom., educt) | ||
| 1H-NMR: 9,10-Dihydro-9,10-ethanoanthracene-11,12-trans-dicarboxylic acid diethyl ester | |||
| 250 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.23 | t (3J = 7.2 Hz) | 6 H | CH3 ethyl |
| 3.45 | m | 2 H | 11-H, 12-H (-CH-COO-) |
| 4.08 | m | 4 H | CH2 ethyl |
| 4.75 | m | 2 H | 9-H, 10-H |
| 7.09-7.38 | m | 8 H | CH (arom.) |
| >7.4 | CH (arom., educt) | ||