| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| Video |
|
|
|
; Side reactions |
Chromatogram |
| GC: crude product | |
| column | SE 54, L=25 m, d=0.32 mm, film=0.25 µm (Macherey & Nagel) |
| inlet | injector: 250°C, split injection 1:20 |
| carrier gas | N2, pre-column pressure 62 kPa |
| oven | 100°C (1 min), 10°C/min --> 250°C (30 min) |
| detector | FID, 275°C |
| integration | percent concentration calculated from relative peak area |
| GC: pure product | |
| column | SE 54, L=25 m, d=0.32 mm, film=0.25 µm (Macherey & Nagel) |
| inlet | injector: 250°C, split injection 1:20 |
| carrier gas | N2, pre-column pressure 62 kPa |
| oven | 100°C (1 min), 10°C/min --> 250°C (30 min) |
| detector | FID, 275°C |
| integration | percent concentration calculated from relative peak area |