| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 62.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 14.1 | CH3 ethyl | ||
| 24.6 | C1 | ||
| 26.3 | C4, tert-butyl-CH3 | ||
| 44.3 | C3 | ||
| 214.3 | C2 | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: Pinacolone | |||
| 62.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 14.1 | CH3 ethyl | ||
| 24.6 | C1 | ||
| 26.3 | C4, tert-butyl-CH3 | ||
| 44.3 | C3 | ||
| 214.3 | C2 | ||
| 76.5-77.5 | CDCl3 | ||