NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
H
2
O
2
/ lipase
; Side reactions
Chromatogram
GC: pure product
column
SE-54, L= 25 m, ID 0.32 mm, DF 0.25 �m (Macherey & Nagel)
inlet
Gerstel KAS, injector: 250�C, split injection 1:20, 1 �L
carrier gas
N2, pre-column pressure 62 kPa, 1.04 mL/min
oven
80 �C (1 min), 5�C/min --> 250�C (30 min)
detector
FID, 275 �C
integration
percent concentration calculated from relative peak area
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pages/experiment.php: November 09, 2022
views/chromatogram.php: November 09, 2022