| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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|
; Side reactions |
Chromatogram |
| GC: pure product | |
| column | SE-54, L= 25 m, ID 0.32 mm, DF 0.25 µm (Macherey & Nagel) |
| inlet | Gerstel KAS, injector: 250°C, split injection 1:20, 1 µL |
| carrier gas | N2, pre-column pressure 62 kPa, 1.04 mL/min |
| oven | 80 °C (1 min), 5°C/min --> 250°C (30 min) |
| detector | FID, 275 °C |
| integration | percent concentration calculated from relative peak area |