| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 13.9 | C10 | ||
| 22.4 | C9 | ||
| 25.0 | C5 | ||
| 27.9-29.0 | C6, C7, C8 | ||
| 31.5 | C3 | ||
| 35.4 | C2 | ||
| 80.9 | C4 | ||
| 177.1 | C1 (O-C(=O)-) | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: gamma-Decalactone | |||
| 125.7 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 13.9 | C10 | ||
| 22.4 | C9 | ||
| 25.0 | C5 | ||
| 27.9-29.0 | C6, C7, C8 | ||
| 31.5 | C3 | ||
| 35.4 | C2 | ||
| 80.9 | C4 | ||
| 177.1 | C1 (O-C(=O)-) | ||
| 76.5-77.5 | CDCl3 | ||