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NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
Cyclopentanone-2-carboxylic acid ethyl ester + Methyl vinyl ketone
FeCl3· 6 H2O
reacts to
 2-(3-Oxobutyl)cyclopentanone-2-carboxylic acid ethyl ester ; Side reactions

Equipment

Batch scale: 0.01 mol 0.1 mol Cyclopentanone-2-carboxylic acid ethyl ester
two-necked flask 10 mL two-necked flask 10 mL protective gas piping protective gas piping
addition funnel with pressure balance addition funnel with pressure balance heatable magnetic stirrer with magnetic stir bar heatable magnetic stirrer with magnetic stir bar
vacuum pump vacuum pump microdistillation apparatus microdistillation apparatus
water bath water bath oil bath oil bath
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