| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| + |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 122.0 | C2 | ||
| 128.3 | C2', C3', C5', C6' (1-phenyl) or (3-phenyl) | ||
| 128.4 | C2', C3', C5', C6' (1-phenyl) or (3-phenyl) | ||
| 128.5 | C2', C3', C5', C6' (1-phenyl) or (3-phenyl) | ||
| 128.9 | C2', C3', C5', C6' (1-phenyl) or (3-phenyl) | ||
| 130.4 | C4' (3-phenyl) | ||
| 132.7 | C4' (1-phenyl) | ||
| 134.8 | C1' (3-phenyl) | ||
| 138.1 | C1' (1-phenyl) | ||
| 144.7 | C3 | ||
| 190.4 | C1 (C=O) | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: Benzalacetophenone | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 122.0 | C2 | ||
| 128.3 | C2', C3', C5', C6' (1-phenyl) or (3-phenyl) | ||
| 128.4 | C2', C3', C5', C6' (1-phenyl) or (3-phenyl) | ||
| 128.5 | C2', C3', C5', C6' (1-phenyl) or (3-phenyl) | ||
| 128.9 | C2', C3', C5', C6' (1-phenyl) or (3-phenyl) | ||
| 130.4 | C4' (3-phenyl) | ||
| 132.7 | C4' (1-phenyl) | ||
| 134.8 | C1' (3-phenyl) | ||
| 138.1 | C1' (1-phenyl) | ||
| 144.7 | C3 | ||
| 190.4 | C1 (C=O) | ||
| 76.5-77.5 | CDCl3 | ||