| Overview |
| Instructions |
| Operating scheme |
| Substances |
| - Substances required |
| - Substances produced |
| - Data availability |
| - Effect factors TRGS 600 |
| Equipment |
| Evaluation |
| Analytics |
|
|
| + |
|
; Side reactions |
Substances required |
| Educts | Amount | Risk | Safety | |||||
|---|---|---|---|---|---|---|---|---|
| 2,2'-Dihydroxy-1,1'-binaphthyl |
|
2.86 g | H301 H319 EUH- | P301 + 310 P305 + 351 + 338 | ||||
| Reagents | Amount | Risk | Safety | |||||
| (-)-N-Benzylcinchonidinium chloride |
|
2.32 g | H315 H319 H335 EUH- | P261 P305 + 351 + 338 | ||||
| Solvents | Amount | Risk | Safety | |||||
| Acetonitrile |
|
50 mL | H225 H302 + 312 + 332 H319 | P210 P280 P305 + 351 + 338 | ||||
| Methanol |
|
30 mL | H225 H331 H311 H301 H370 | P210 P260 P280 P301 + 310 P311 | ||||
| Acetic acid ethyl ester |
|
90 mL | H225 H319 H336 EUH066 | P210 P261 P305 + 351 + 338 | ||||
| Water |
| H- EUH- | P- | |||||
| Others | Amount | Risk | Safety | |||||
| Hydrochloric acid 2N |
|
90 mL | ||||||
| Sodium chloride |
|
~7 g | ||||||
| Sodium carbonate |
| H319 EUH- | P305 + 351 + 338 | |||||
| Sodium sulfate |
| |||||||
| Silica gel |
|
