| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 13.8 | CH3 ethyl | ||
| 20.6 | C4 | ||
| 27.1 | C5 | ||
| 37.7 | C3 | ||
| 54.4 | C1 | ||
| 60.9 | CH2 ethyl | ||
| 169.1 | -C(=O)O- | ||
| 211.9 | C2 | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: Cyclopentanone-2-carboxylic acid ethyl ester | |||
| 75.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 13.8 | CH3 ethyl | ||
| 20.6 | C4 | ||
| 27.1 | C5 | ||
| 37.7 | C3 | ||
| 54.4 | C1 | ||
| 60.9 | CH2 ethyl | ||
| 169.1 | -C(=O)O- | ||
| 211.9 | C2 | ||
| 76.5-77.5 | CDCl3 | ||