| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
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; Side reactions |
Acid catalyzed acetalisation of 3-nitrobenzaldehyde with ethanediol to the correspondent 1,3-dioxolane |
| Reaction type: | reaction of the carbonyl group in aldehydes, acetalisation |
| Substance classes: | aldehyde, acetal, alcohol, protecting group, acid catalyst |
| Techniques: | microwave-assisted reaction, stirring with magnetic stir bar, heating under reflux, distillation, introduction of gas, shaking out, extracting, evaporating with rotary evaporator, filtering, recrystallizing |
| Degree of difficulty: | Medium |