| Overview |
| Instructions |
| Operating scheme |
| Substances |
| - Substances required |
| - Substances produced |
| - Data availability |
| - Effect factors TRGS 600 |
| - Stoichiometry |
| Equipment |
| Evaluation |
| Analytics |
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| + |
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; Side reactions |
Substances required |
| Educts | Amount | Risk | Safety | ||||||
|---|---|---|---|---|---|---|---|---|---|
| 3-Nitrobenzaldehyde |
|
15.1 g | H302 H411 | P273 | |||||
| 1,2-Ethanediol |
|
9.32 g | H302 | P301 + 312 | |||||
| Catalyst | Amount | Risk | Safety | ||||||
| 4-Toluenesulfonic acid monohydrate |
|
1.0 g | H315 H319 H335 | P261 P305 + 351 + 338 | |||||
| Solvents | Amount | Risk | Safety | ||||||
| tert-Butyl methyl ether |
|
240 mL | H225 H315 | P210 | |||||
| Petroleum ether (40-60) |
|
70 mL | H225 H304 H315 H336 H411 EUH- | P210 P261 P273 P301 + 310 P331 | |||||
| Water |
|
200 mL | H- EUH- | P- | |||||
| Others | Amount | Risk | Safety | ||||||
| Ice |
|
H- EUH- | P- | ||||||
| Sodium disulfite |
|
~13 g | H302 H318 EUH031 | P280 P305 + 351 + 338 P313 | |||||
| Sodium sulfate |
|
~15 g | |||||||
| Solvents for analysis | Amount | Risk | Safety | ||||||
| Acetic acid ethyl ester |
| H225 H319 H336 EUH066 | P210 P261 P305 + 351 + 338 |
