| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - IR |
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; Side reactions |
Chromatogram |
| GC: crude product | |
| Coluna | Zebron ZB-1, L=30 m, d=0.32 mm, film=0.25 µm |
| inlet | injector: 210°C, split injection, 1 µl |
| Gás carreador | H2, pre-column pressure 50 kPa |
| Forno | 70°C (2 min), 10°C/min --> 300°C (10 min) |
| Detector | FID, 310°C |
| integration | a concentração percentual foi calculada a partir da área dos picos |