NOP - Sustainability in the organic chemistry lab course

Pinacol

H₂SO₄

reacts to

Pinacolona

; Side reactions

Chromatogram

crude product chromatogram

GC: crude product
Coluna	SE-54, L= 25 m, ID 0.32 mm, DF 0.25 µm (Macherey & Nagel)
inlet	Gerstel KAS, injector: 250°C, split injection 1:20, 2 µL
Gás carreador	N2, pre-column pressure 62 kPa, 1.04 mL/min
Forno	50 °C
Detector	FID, 275 °C
integration	a concentração percentual foi calculada a partir da área dos picos

pure product chromatogram

GC: pure product
Coluna	SE-54, L= 25 m, ID 0.32 mm, DF 0.25 µm (Macherey & Nagel)
inlet	Gerstel KAS, injector: 250°C, split injection 1:20, 2 µL
Gás carreador	N2, pre-column pressure 62 kPa, 1.04 mL/min
Forno	50 °C
Detector	FID, 275 °C
integration	a concentração percentual foi calculada a partir da área dos picos

pure product chromatogram

: pure product
Coluna	SE-54, L= 25 m, ID 0.32 mm, DF 0.25 µm (Macherey & Nagel)
inlet	Gerstel KAS, injector: 250°C, split injection 1:20, 2 µL
Gás carreador	N2, pre-column pressure 62 kPa, 1.04 mL/min
Forno	50 °C
Detector	FID, 275 °C
integration	a concentração percentual foi calculada a partir da área dos picos