| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
1H-NMR |
| 1H-NMR: 2-Nitrofenol | |||
| 300 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 6.99 | dt | 1 H | 4-H |
| 7.15 | ddd | 1 H | 6-H |
| 7.58 | dt | 1 H | 5-H |
| 8.10 | dd | 1 H | 3-H |
| 10.58 | s | 1 H | OH |
| 7.26 | 1 H | CHCl3 | |
| 1H-NMR: 4-Nitrofenol | |||
| 300 MHz, Me2C=O-d6 | |||
| delta [ppm] | mult. | atoms | assignment |
| 7.02 | d (XX') | 2 H | 2-H, 6-H |
| 8.15 | d (AA') | 2 H | 3-H, 5-H |
| 9.80 | s | 1 H | OH |
| 2.04 | Me2C=O | ||
| 3.1 | H2O | ||
| 7.26 | 1 H | CHCl3 | |