| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
13C-NMR |
| 13C-NMR: 2-Methyl-1,3-dioxolane-2-acetic acid ethyl ester | |||
| 250 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 14.1 | CH3 ethyl | ||
| 24.5 | CH3 dioxolane | ||
| 44.2 | CH2 alpha | ||
| 60.5 | CH2 ethyl | ||
| 64.7 | CH2-CH2 dioxolane | ||
| 107.6 | Cquart. dioxolane | ||
| 169.4 | C(=O)O ester | ||
| 76.5-77.5 | CDCl3 | ||