| Overview |
| Instructions |
| Operating scheme |
| Substances |
| - Substances required |
| - Substances produced |
| - Data availability |
| - Effect factors TRGS 600 |
| Equipment |
| Evaluation |
| Analytics |
| + |
|
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| + |
|
; Side reactions |
Substances required |
| Educts | Amount | Risk | Safety | ||||||
|---|---|---|---|---|---|---|---|---|---|
| Acetoacetic acid ethyl ester |
|
1.30 g | H319 | P305 + 351 + 338 | |||||
| 1,2-Ethanediol |
|
0.745 g | H302 | P301 + 312 | |||||
| Catalyst | Amount | Risk | Safety | ||||||
| Montmorillonite K 10 |
|
0.60 g | H- EUH- | P- | |||||
| Solvents | Amount | Risk | Safety | ||||||
| Cyclohexane |
|
60 mL | H225 H304 H315 H336 H410 | P210 P233 P240 P273 P301 + 310 P302 + 352 P331 P403 + 235 | |||||
| Ethanol |
|
50 mL | H225 H302 H371 EUH- | P210 P260 | |||||
| Others | Amount | Risk | Safety | ||||||
| 2,4-Dinitrophenyl hydrazine |
|
2 g | H228 H302 | P210 | |||||
| Sulfuric acid (conc.) |
|
10 mL | H314 H290 EUH- | P280 P301 + 330 + 331 P305 + 351 + 338 P309 + 310 | |||||
| Molecular sieve 4A |
|
5 g | H315 H319 H335 | P261 P305 + 351 + 338 |
