| Overview |
| Instructions |
| Operating scheme |
| Substances |
| - Substances required |
| - Substances produced |
| - Data availability |
| - Effect factors TRGS 600 |
| - Stoichiometry |
| Equipment |
| Evaluation |
| Analytics |
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; Side reactions |
Substances required |
| Educts | Amount | Risk | Safety | ||||||
|---|---|---|---|---|---|---|---|---|---|
| 3-Nitrobenzaldehyde |
|
15.1 g | H302 H411 | P273 | |||||
| 1,2-Ethanediol |
|
6.83 g | H302 | P301 + 312 | |||||
| Catalyst | Amount | Risk | Safety | ||||||
| 4-Toluenesulfonic acid monohydrate |
|
0.19 g | H315 H319 H335 | P261 P305 + 351 + 338 | |||||
| Solvents | Amount | Risk | Safety | ||||||
| Cyclohexane |
|
~ 230 mL | H225 H304 H315 H336 H410 | P210 P233 P240 P273 P301 + 310 P302 + 352 P331 P403 + 235 | |||||
| tert-Butyl methyl ether |
|
230 mL | H225 H315 | P210 | |||||
| Others | Amount | Risk | Safety | ||||||
| Sodium disulfite |
|
~ 13 g | H302 H318 EUH031 | P280 P305 + 351 + 338 P313 | |||||
| Sodium sulfate |
|
~ 5 g | |||||||
| Molecular sieve 4A |
|
0 g | H315 H319 H335 | P261 P305 + 351 + 338 | |||||
| Solvents for analysis | Amount | Risk | Safety | ||||||
| tert-Butyl methyl ether |
|
5 mL | H225 H315 | P210 |
