| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
1H-NMR |
| 1H-NMR: crude product | |||
| 400 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.62 | s | 3 H | CH3 |
| 1.84 | s | 3 H | CH3 |
| 4.84 | s | 1 H | CH-O (educt) |
| 5.53 | s | 2 H | CH-O (product) |
| 6.8-7.2 | m | 10 H | CH (arom., product) |
| 7.2-7.4 | m | 10 H | CH (arom., educt) |
| 7.26 | s | 1 H | CHCl3 |
| 1H-NMR: cis-2,2-Dimethyl-4,5-diphenyl-1,3-dioxolane | |||
| 300 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.62 | s | 3 H | CH3 |
| 1.84 | s | 3 H | CH3 |
| 4.84 | s | 1 H | CH-O (educt) |
| 5.53 | s | 2 H | CH-O (product) |
| 6.8-7.2 | m | 10 H | CH (arom., product) |
| 7.2-7.4 | m | 10 H | CH (arom., educt) |
| 7.26 | s | 1 H | CHCl3 |