NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
+
montmorillonite
K-10
cyclohexane
+
; Side reactions
13
C-NMR
13
C-NMR: N-[(5R)-2-Methyl-5-(1-methylethenyl)-2-cyclohexen-1-ylidene]benzylamine
250 MHz, CDCl
3
delta [ppm]
assignment
18.4
CH
3
20.7
CH
3
30.7
CH
2
ring
32.1
CH
2
ring
41.7
CH isopropenyl
54.0
CH
2
benzyl
110.0
=CH
2
126.4
CH arom.
127.5
CH arom.
128.3
CH arom.
134.2
CH=C ring
135.8
-C(CH
3
)=C ring
140.9
C quart. arom.
148.1
-C(CH
3
)=C isopropenyl
167.5
C=N ring
76.5-77.5
CDCl
3
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pages/experiment.php: November 09, 2022
views/cnmr.php: November 09, 2022