NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
+
montmorillonite
K-10
cyclohexane
+
; Side reactions
1
H-NMR
1
H-NMR: crude product
250 MHz, CDCl
3
delta [ppm]
mult.
atoms
assignment
1.77
s
3 H
CH
3
1.96
s
3 H
CH
3
2.0-2.6
m
4 H
CH
2
ring
2.90
m
1 H
tert. -H
4.69
m
2 H
CH
2
benzyl
4.80
m
2 H
CH
2
=C
6.29
m
1 H
CH=C ring
7.2-7.5
m
5 H
CH (arom.)
1
H-NMR: N-[(5R)-2-Methyl-5-(1-methylethenyl)-2-cyclohexen-1-ylidene]benzylamine
250 MHz, CDCl
3
delta [ppm]
mult.
atoms
assignment
1.77
s
3 H
CH
3
1.96
s
3 H
CH
3
2.0-2.6
m
4 H
CH
2
ring
2.90
m
1 H
tert. -H
4.69
m
2 H
CH
2
benzyl
4.80
m
2 H
CH
2
=C
6.29
m
1 H
CH=C ring
7.2-7.5
m
5 H
CH (arom.)
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pages/experiment.php: November 09, 2022
views/hnmr.php: November 09, 2022