| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
Chromatogram |
| GC: crude product | |
| column | CB-WAX 57 CB, L=50 m, d=0.31 mm, film=1.2 µm |
| inlet | split injection, 0.05 µL |
| carrier gas | He, pre-column pressure 50 kPa |
| oven | 30°C (8 min), 4°C/min --> 50°C, 0.5°C/min --> 68°C, 10°C/min --> 170°C (20 min) |
| detector | FID, 300°C, H2 93 kPa, synth. air 300 kPa |
| integration | percent concentration calculated from relative peak area |
| GC: pure product | |
| column | CB-WAX 57 CB, L=50 m, d=0.31 mm, film=1.2 µm |
| inlet | split injection, 0.05 µL |
| carrier gas | He, pre-column pressure 50 kPa |
| oven | 30°C (8 min), 4°C/min --> 50°C, 0.5°C/min --> 68°C, 10°C/min --> 170°C (20 min) |
| detector | FID, 300°C, H2 93 kPa, synth. air 300 kPa |
| integration | percent concentration calculated from relative peak area |