NOP-Nr:
Overview
Instructions
Operating scheme
Substances
Equipment
Evaluation
Analytics
- Chromatogram
-
1
H-NMR
-
13
C-NMR
- IR
+
4-toluenesulfonic
acid
cyclohexane
+
; Side reactions
13
C-NMR
13
C-NMR: Propionic acid butyl ester
250 MHz, CDCl
3
delta [ppm]
assignment
9.2
C3 (propanoic acid residue)
13.7
C4 (butyl)
19.1
C3 (butyl)
27.6
C2 (propanoic acid residue)
30.7
C2 (butyl)
64.2
C1 (butyl)
174.6
C=O
76.5-77.5
CDCl
3
26.9
CH
2
(cyclohexane)
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pages/experiment.php: November 09, 2022
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