| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
Chromatogram |
| GC: crude product | |
| column | Zebron ZB-1, L=15 m, d=0.25 mm, film=0.25 µm |
| inlet | injector: 270°C, split injection 21:1, 0.3 µL |
| carrier gas | He, pre-column pressure 100 kPa |
| oven | 60°C |
| detector | FID, 250°C, H2 29 mL/min, synth. air 333 mL/min |
| integration | percent concentration calculated from relative peak area |
| : pure product | |
| column | Zebron ZB-1, L=15 m, d=0.25 mm, film=0.25 µm |
| inlet | injector: 270°C, split injection 21:1, 0.3 µL |
| carrier gas | He, pre-column pressure 100 kPa |
| oven | 60°C |
| detector | FID, 250°C, H2 29 mL/min, synth. air 333 mL/min |
| integration | percent concentration calculated from relative peak area |