| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: (-)-Isoborneol and (+)-borneol, mixture | |||
| 250 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 11.33 | CH3 (1-methyl, isoborneol) | ||
| 20.12 | CH3 (7-methyl, isoborneol) | ||
| 20.49 | CH3 (7-methyl, isoborneol) | ||
| 27.25 | C5 (CH2, isoborneol) | ||
| 33.92 | C6 (CH2, isoborneol) | ||
| 40.41 | C3 (CH2, isoborneol) | ||
| 45.05 | C4 (CH, isoborneol) | ||
| 46.35 | C7 (C-quart., isoborneol) | ||
| 48.97 | C1 (C-quart., isoborneol) | ||
| 79.92 | C2 (CHOH, isoborneol) | ||
| 13.34 | CH3 (1-methyl, borneol) | ||
| 18.69 | CH3 (7-methyl, borneol) | ||
| 20.20 | CH3 (7-methyl, borneol) | ||
| 25.93 | C6 (CH2, borneol) | ||
| 28.29 | C5 (CH2, borneol) | ||
| 39.04 | C3 (CH2, borneol) | ||
| 45.11 | C4 (CH, borneol) | ||
| 48.03 | C7 (C-quart., borneol) | ||
| 49.50 | C1 (C-quart., borneol) | ||
| 77.21 | C2 (CHOH, borneol) | ||
| 76.5-77.5 | CDCl3 | ||