| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 125 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 28.6 | C5, C5', C7, C7' | ||
| 31.9 | C1, C1', C-3, C3' | ||
| 37.3 | C6, C6' | ||
| 39.6 | C4, C4', C8, C8', C9, C9', C10, C10' | ||
| 133.1 | C2, C2' | ||
| 76.5-77.5 | CDCl3 | ||
| 13C-NMR: Adamantanylideneadamantane | |||
| 125 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 28.6 | C5, C5', C7, C7' | ||
| 31.9 | C1, C1', C-3, C3' | ||
| 37.3 | C6, C6' | ||
| 39.6 | C4, C4', C8, C8', C9, C9', C10, C10' | ||
| 133.1 | C2, C2' | ||
| 76.5-77.5 | CDCl3 | ||