| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
1H-NMR |
| 1H-NMR: crude product | |||
| 500 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.63-1.69 | m | 8 H | CH2 |
| 1.79-1.86 | m | 12 H | CH2 |
| 1.90 | m | 4 H | 5-H, 5'-H, 7-H, 7'-H |
| 2.88 | m | 4 H | 1-H, 1'-H, 3-H, 3'-H |
| 7.26 | CHCl3 | ||
| 1H-NMR: Adamantanylideneadamantane | |||
| 500 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.63-1.69 | m | 8 H | CH2 |
| 1.79-1.86 | m | 12 H | CH2 |
| 1.90 | m | 4 H | 5-H, 5'-H, 7-H, 7'-H |
| 2.88 | m | 4 H | 1-H, 1'-H, 3-H, 3'-H |
| 7.26 | CHCl3 | ||