| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
| + |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 125 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 25.2 | C4 | ||
| 27.3 | C3, C5 | ||
| 32.9 | C1 | ||
| 39.6 | C2, C6 | ||
| 76.5-77.5 | CDCl3 | ||
| -66.3 | CH2I2 | ||
| 13C-NMR: Iodocyclohexane | |||
| 125 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 25.2 | C4 | ||
| 27.3 | C3, C5 | ||
| 32.9 | C1 | ||
| 39.6 | C2, C6 | ||
| 76.5-77.5 | CDCl3 | ||
| -66.3 | CH2I2 | ||