| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
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; Side reactions |
1H-NMR |
| 1H-NMR: crude product | |||
| 500 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.32-1.42 | m | 3 H | CH2 |
| 1.58-1.69 | m | 3 H | CH2 |
| 1.89-2.00 | m | 2 H | CH2 |
| 2.10-2.18 | m | 2 H | CH2 |
| 4.30-4.38 | m | 1 | 1-H (-CH-I) |
| 7.26 | CHCl3 | ||
| 3.87 | CH2I2 | ||
| 1H-NMR: Iodocyclohexane | |||
| 500 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.32-1.42 | m | 3 H | CH2 |
| 1.58-1.69 | m | 3 H | CH2 |
| 1.89-2.00 | m | 2 H | CH2 |
| 2.10-2.18 | m | 2 H | CH2 |
| 4.30-4.38 | m | 1 | 1-H (-CH-I) |
| 7.26 | CHCl3 | ||
| 3.87 | CH2I2 | ||