| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 62.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 14.1 | CH3 (ethyl ester) | ||
| 30.9 | C3 | ||
| 35.9 | C2 | ||
| 60.3 | CH2 (ethyl ester) | ||
| 126.2 | C4' (CH arom.) | ||
| 128.2-128.4 | CH arom. | ||
| 140.5 | C quart. arom. | ||
| 172.9 | C1 (-COO-) | ||
| 76.5-77.5 | CDCl3 | ||
| 32.0 | C2 (3-phenylpropanol) | ||
| 34.1 | C3 (3-phenylpropanol) | ||
| 62.1 | CH2OH (3-phenylpropanol) | ||
| 125.8 | C4' (CH arom., 3-phenylpropanol) | ||
| 128.2-128.4 | CH arom., 3-phenylpropanol | ||
| 141.8 | C quart. arom. (3-phenylpropanol) | ||
| 13C-NMR: 3-Phenylpropionic acid ethyl ester | |||
| 62.5 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 14.1 | CH3 (ethyl ester) | ||
| 30.9 | C3 | ||
| 35.9 | C2 | ||
| 60.3 | CH2 (ethyl ester) | ||
| 126.2 | C4' (CH arom.) | ||
| 128.2-128.4 | CH arom. | ||
| 140.5 | C quart. arom. | ||
| 172.9 | C1 (-COO-) | ||
| 76.5-77.5 | CDCl3 | ||
| 32.0 | C2 (3-phenylpropanol) | ||
| 34.1 | C3 (3-phenylpropanol) | ||
| 62.1 | CH2OH (3-phenylpropanol) | ||
| 125.8 | C4' (CH arom., 3-phenylpropanol) | ||
| 128.2-128.4 | CH arom., 3-phenylpropanol | ||
| 141.8 | C quart. arom. (3-phenylpropanol) | ||