| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
1H-NMR |
| 1H-NMR: crude product | |||
| 250 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.25 | t (3J = 7.1 Hz) | 3 H | CH3 ethyl |
| 2.63 | m | 2 H | 2-H |
| 2.97 | m | 2 H | 3-H |
| 4.14 | q (3J = 7.1 Hz) | 2 H | CH2 ethyl |
| 7.17-7.35 | m | 5 H | CH (arom.) |
| 1.91 | m | 2 H | 2-H (3-phenylpropanol) |
| 2.73 | m | 2 H | 3-H (3-phenylpropanol) |
| 3.68 | t (3J = 6.4 Hz) | 2 H | 1-H (3-phenylpropanol) |
| 1H-NMR: 3-Phenylpropionic acid ethyl ester | |||
| 250 MHz, CDCl3 | |||
| delta [ppm] | mult. | atoms | assignment |
| 1.25 | t (3J = 7.1 Hz) | 3 H | CH3 ethyl |
| 2.63 | m | 2 H | 2-H |
| 2.97 | m | 2 H | 3-H |
| 4.14 | q (3J = 7.1 Hz) | 2 H | CH2 ethyl |
| 7.17-7.35 | m | 5 H | CH (arom.) |
| 1.91 | m | 2 H | 2-H (3-phenylpropanol) |
| 2.73 | m | 2 H | 3-H (3-phenylpropanol) |
| 3.68 | t (3J = 6.4 Hz) | 2 H | 1-H (3-phenylpropanol) |