| Overview |
| Instructions |
| Operating scheme |
| Substances |
| Equipment |
| Evaluation |
| Analytics |
| - Chromatogram |
| - 1H-NMR |
| - 13C-NMR |
| - IR |
|
|
|
; Side reactions |
13C-NMR |
| 13C-NMR: crude product | |||
| 125 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 24.3 | C4, C5 | ||
| 32.8 | C3, C6 | ||
| 75.6 | C2, C1 | ||
| 76.5-77.5 | CDCl3 | ||
| 21.3 | C4 (byproduct, 1-formate) | ||
| 23.8 | C5 (byproduct, 1-formate) | ||
| 29.9 | C6 (byproduct, 1-formate) | ||
| 33.0 | C3 (byproduct, 1-formate) | ||
| 72.6 | C2 (byproduct, 1-formate) | ||
| 78.1 | C1 (byproduct, 1-formate) | ||
| 171.5 | C(=O)O (byproduct, 1-formate) | ||
| 13C-NMR: trans-1,2-Cyclohexanediol | |||
| 125 MHz, CDCl3 | |||
| delta [ppm] | assignment | ||
| 24.3 | C4, C5 | ||
| 32.8 | C3, C6 | ||
| 75.6 | C2, C1 | ||
| 76.5-77.5 | CDCl3 | ||
| 21.3 | C4 (byproduct, 1-formate) | ||
| 23.8 | C5 (byproduct, 1-formate) | ||
| 29.9 | C6 (byproduct, 1-formate) | ||
| 33.0 | C3 (byproduct, 1-formate) | ||
| 72.6 | C2 (byproduct, 1-formate) | ||
| 78.1 | C1 (byproduct, 1-formate) | ||
| 171.5 | C(=O)O (byproduct, 1-formate) | ||